HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 4-tert.-Octyl-2,6-dimethyl-3-hydroxyphenylacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 86734106 | HCID 86734106 | — |
| Product | 4-tert.-Octyl-2,6-dimethyl-3-hydroxyphenylacetic acid | HCID 86734105 | — |
Reaction Steps
This compound was made in a similar manner to the method disclosed in Example 5 by hydrolyzing 4-tert.-octyl-2,6-dimethyl-3-hydroxyphenylacetonitrile with sodium hydroxide in aqueous ethylene glycol. After crystallization from toluene 4-tert.-octyl-2,6-dimethyl-3-hydroxyphenylacetic acid melted at 157° to 159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04187246 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-e852a8053ed84628a629f65553abd6db |
| Source note | uspto-grants-1980_02 |