Sodium Bicarbonate → HCID 23666533, compound

Participants

Reaction Steps

An aqueous solution (1.63 ml.) of 1 M-sodium hydrogen carbonate was added to a stirred suspension of powdered α-(1-benzyl-1,2-dihydro-2-oxoquinol-4-yl)propionic acid (0.50 g.) in distilled water (3.37 ml.), and the mixture was stirred overnight, at ambient temperature. The solid which had formed was separated and dried in vacuo over phosphorus pentoxide to give sodium α-(1-benzyl-1,2-dihydro-2-oxoquinol-4-yl)-propionate (0.52 g.) as its monohydrate (m.p., indefinite;

Provenance & Evidence