HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boc-L-Valine → HCID 91979019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boc-L-Valine | HCID 83693 | — |
| Reactant | 34290-71-6 | HCID 13273161 | — |
| Product | HCID 91979019 | HCID 91979019 | — |
Reaction Steps
Boc-Val-OH (52.1 g, 240 mmol) was reacted with II (53.4 g, 240 mmol) by the mixed anhydride method as described for the preparation of I in part (a). The resulting oil showed a single spot on TLC; yield 64.0 g (69%), Rf1 0.69.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04187852 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-3c20e92bf6a14814a14372a85c123524 |
| Source note | uspto-grants-1980_02 |