HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20351264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20351264 | HCID 20351264 | — |
Reaction Steps
0.2 mol of hydrazine hydrate is run, whilst stirring, into 0.2 mol of diethyl phosphite. During the addition, the mixture is heterogeneous and its temperature rises to 70° C. Ten minutes after the end of the addition, the mixture becomes homogeneous. The mixture is stirred for two hours, and the alcohol and water are then driven off in vacuo at 80° C. A clear oil remains.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04188381 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-153e7487b02640b4b41b0a928d569b06 |
| Source note | uspto-grants-1980_02 |