Hydrazine hydrate (1:1) → HCID 20351264, compound

HRID 1448940Notes

Reaction equation

HRID 1448940 reaction equation
O.[NH2:2][NH2:3].[P:4]([O-:11])([O:8]CC)[O:5][CH2:6][CH3:7]>O>[CH2:6]([O:5][P:4]([O-:11])[O-:8])[CH3:7].[NH3+:2][NH2:3].[NH3+:2][NH2:3]

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 3780918Diethylphosphite

Product 1

HCID 20351264HCID 20351264, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

0.2 mol of hydrazine hydrate is run, whilst stirring, into 0.2 mol of diethyl phosphite. During the addition, the mixture is heterogeneous and its temperature rises to 70° C. Ten minutes after the end of the addition, the mixture becomes homogeneous. The mixture is stirred for two hours, and the alcohol and water are then driven off in vacuo at 80° C. A clear oil remains.

Workup

  1. additionDuring the addition
  2. customrises to 70° C
  3. additionTen minutes after the end of the addition
  4. customare then driven off in vacuo at 80° C

Sources & evidence

ORD record
ord-153e7487b02640b4b41b0a928d569b06
Source dataset
uspto-grants-1980_02
Patent number
US04188381

Reaction notes

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