Methyl Chloride → HCID 20351236, compound

Participants

Reaction Steps

Into 14.4 g (0.05 m) of dioctyl ethyl phosphine, placed in the bubbler reactor described in Example 2, methyl chloride was introduced at 130° C. for 4 hours. The degree of weight gain observed corresponded to a quantitative formation of the desired product; a colorless, waxy solid at room temperature. In the nmr spectrum of this product, the α-meythyl doublet appears at 1.93 ppm (JP-C 14 cps).

Provenance & Evidence