HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylthio)benzaldehyde → HCID 70592102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylthio)benzaldehyde | HCID 286443 | — |
| Reactant | 2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- | HCID 643756 | — |
| Reactant | Ethyl 4-(1,3-dioxoisoindolin-2-YL)-3-oxobutanoate | HCID 701239 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70592102 | HCID 70592102 | — |
Reaction Steps
A solution of 10 g of 2-methylmercapto-benzaldehyde (77% pure), 14 g of phthalimidoacetoacetic acid ethyl ester and 6.5 g of β-aminocrotonic acid ethyl ester in 100 ccs of ethanol is heated under reflux for 2×24 hours and, after subsequent cooling, the precipitate is filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04188395 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-d6ca04bf81634475ba13bc5feacc68c0 |
| Source note | uspto-grants-1980_02 |