HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 70591792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Ethyl 4-(1,3-dioxoisoindolin-2-YL)-3-oxobutanoate | HCID 701239 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 70591792 | HCID 70591792 | — |
Reaction Steps
7.5 g of 4-nitrobenzaldehyde, 28 g of γ-phthalimidoacetoacetic acid ethyl ester and 7 ccs of concentrated ammonia in 120 ccs of ethanol are heated to the boil under reflux for 60 hours and the product is filtered off after cooling on ice.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04188395 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-5205feddbabe449fa1be8fca1de6508a |
| Source note | uspto-grants-1980_02 |