HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 20350133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 14416083 | HCID 14416083 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20350133 | HCID 20350133 | 79% |
Reaction Steps
6-Chloro-9-(2,6-dichlorobenzyl)purine (314 mg), 322 mg of 70% aqueous ethylamine and 25 ml of methanol were treated in the same manner as Example 2, whereby 255 mg (yield 79%) of 9-(2,6-dichlorobenzyl)-6-ethylaminopurine was obtained as needles melting at 222°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04189485 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-3e6954e56acc44758f472f0fe7697924 |
| Source note | uspto-grants-1980_02 |