HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 20349084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Benzenamine, N-hydroxy-4-methyl-3-nitro- | HCID 5488054 | — |
| Product | HCID 20349084 | HCID 20349084 | — |
Reaction Steps
A solution of methyl isocyanate (4.1 g; 4.6 ml.) in diethyl ether (20 ml.) was added with stirring to a solution of N-(3-nitro-4-methylphenyl)-hydroxylamine (12.0 g.) in ether (70 ml.) at room temperature over a period of about 10 minutes. The yellow precipitate 1-methyl-3-(3'-nitro-4'-methylphenyl)-3-hydroxyurea which formed was filtered and air dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04190431 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-28f17e67d1484fa2a7a55a0ff58b13f7 |
| Source note | uspto-grants-1980_02 |