HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tiflamizole → HCID 86736848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tiflamizole | HCID 44188 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86736848 | HCID 86736848 | — |
Reaction Steps
A mixture of 4,5l -bis(4-fluorophenyl)-2-(1,1,2,2-tetrafluoroethylsulfonyl)imidazole (5.0 g., 0.0119 mole), sodium methoxide (0.6 g., 0.0111 mole) and ether (300 ml.) is stirred overnight at room temperature. The solid is collected and washed with ether to give 2.1 g. of the sodium salt of 4,5-bis(4-fluorophenyl)-2-(1,1,2,2-tetrafluoroethylsulfonyl)imidazole, m.p. 290°-292°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04190666 |
| Source dataset | uspto-grants-1980_02 |
| ORD ID | ord-bf450b271feb4328b14caf405da01dd2 |
| Source note | uspto-grants-1980_02 |