Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1449440Generated: November 2, 2026

Benzyl Alcohol → HCID 19977709, compound

https://huagongshe.com/reaction/1449440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl AlcoholHCID 244—
ReactantSodium hydrideHCID 24758—
ReactantHCID 19977708HCID 19977708—
SolventTetrahydrofuranHCID 8028—
ProductHCID 19977709HCID 19977709—

Reaction Steps

To benzyl alcohol (Compound II-64) (0.35 g, 0.0016×2.0 mol) in tetrahydrofuran, sodium hydride (0.085 g, (60% in mineral oil), 0.0016×1.3 mol) and 4-ethoxy-6-methyl-2-(methylsulfonyl)pyrimidine (Compound III-44) (0.35 g, 0.0016 mol) prepared as described in Reference synthesis example 1 below were successively added and the solution was allowed to react for about 1 hour at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05599770
Source datasetuspto-grants-1997_02
ORD IDord-dff60029e2a7430f88e578b9650c89ba
Source noteuspto-grants-1997_02