HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21855102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Chloro-6-methyl-2-(methylthio)pyrimidine | HCID 241163 | — |
| Product | HCID 21855102 | HCID 21855102 | — |
Reaction Steps
To sodium hydride (2.75 g (60% in mineral oil), 0.046×1.5 mmol) dissolved in ethanol (20 ml), 4-chloro-6-methyl-2-methylmercaptopyrimidine (Compound IV-7) (8.0 g, 0.046 mmol) was added and the solution was stirred for about 1 hour at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599770 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-482b302b29ce43229a7318e98ca7feb3 |
| Source note | uspto-grants-1997_02 |