HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19978182, compound → HCID 67715282, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19978182 | HCID 19978182 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 67715282 | HCID 67715282 | 78.9% |
Reaction Steps
In 100 ml of 2N hydrochloric acid was suspended 2.0 g of tert-butyl 3,6,6-trimethyl-6,7-dihydro-5H-thiazolo[3,2-a]-pyrimidine-2-carboxylate hydrochloride obtained in Example 119, followed by stirring at room temperature for 7 hours. The precipitated crystals were collected by filtration and washed with diethylether and acetone to obtain 1.3 g of the titled compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599813 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-1af3256b4b78422996db69c62e6e0a43 |
| Source note | uspto-grants-1997_02 |