Glycinamide → HCID 54569709, compound

HRID 1449601Notes

Reaction equation

HRID 1449601 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[N:9]=[C:10]=[S:11].[NH2:12][CH2:13][C:14]([NH2:16])=[O:15]>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Cl:8])[C:3]=1[NH:9][C:10](=[S:11])[NH:12][CH2:13][C:14]([NH2:16])=[O:15]

Participants

3

Reactant 2

HCID 69020GlycinamideHCID 1232391,3-Dichloro-2-isothiocyanatobenzene

Product 1

HCID 54569709HCID 54569709, compound

Procedure

2-[3-(2,6-Dichlorophenyl)-thioureido]-acetamide was prepared by the procedure described in Example 2 using 40.8 g of 2,6-dichlorophenyl-isothiocyanate and 29.6 g of glycinamide. The product was obtained (54 g) as a solid, m.p. 189°-191° C. Mass spectrum (+FAB, [M+H]+) m/z 278/280/282. This intermediate was used in the next paragraph without further purification.

Workup

  1. customThe product was obtained (54 g) as a solid, m.p. 189°-191° C
  2. customThis intermediate was used in the next paragraph without further purification

Sources & evidence

ORD record
ord-901d63f3e3a54feaaf42baf0bd821e0f
Source dataset
uspto-grants-1997_02
Patent number
US05599829

Reaction notes

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