HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycinamide → 2-[3-(2-Chloro-6-methylphenyl)-thioureido]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycinamide | HCID 69020 | — |
| Reactant | 2-Chloro-6-Methylphenyl Isothiocyanate | HCID 3731725 | — |
| Product | 2-[3-(2-Chloro-6-methylphenyl)-thioureido]-acetamide | HCID 54394060 | — |
Reaction Steps
2-[3-(2-Chloro-6-methylphenyl)-thioureido]-acetamide was prepared by the procedure described in Example 2 using 18.3 g of 2-chloro-6-methylphenylisothiocyanate and 12.0 g of glycinamide. 22.8 Grams of the product was obtained, m.p. 161°-163° C. (dec.). This compound was used without further purification in the next paragraph.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599829 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-ce21785bce2a4cc4b0c6bb0b05db383f |
| Source note | uspto-grants-1997_02 |