HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 15334936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15334935 | HCID 15334935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15334936 | HCID 15334936 | 76% |
Reaction Steps
(1.0 g, 3.38 mmole) A solution of 5,7-dichloro-2-(p-chlorophenyl)-indole(in tetrahydrofuran is treated dropwise with 1.0 mL of thionyl chloride, stirred for 16 hours at room temperature, poured over ice and filtered. The filtercake is air-dried to afford the title product as a yellow solid, 0.85 g (76% yield), mp 148°-149° C., identified by IR, 1HNMR and elemental analyses.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599832 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-b7f15e31d354448b85aca017b630bd68 |
| Source note | uspto-grants-1997_02 |