HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropyl iodide → HCID 67721451, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | HCID 9820288 | HCID 9820288 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 67721451 | HCID 67721451 | — |
Reaction Steps
The title compound 8 was obtained as a colorless oil (36 mg, 95%), following a procedure similar to that disclosed in Example 5 except that the compound 6 obtained above (33 mg, 0.1 mmole) was dissolved in acetonitrile (1 ml), and 1,8-diazabicyclo[5.4.0]-7-undecene (40 μl, 0.3 mmole) and then isopropyl iodide (0.19 μl, 1 mmole) were added thereto.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599837 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-95265a8d8af8462aad0a36d5c4179237 |
| Source note | uspto-grants-1997_02 |