Isopropyl iodide → HCID 67721476, compound

Participants

Reaction Steps

The compound 28' obtained obove (87 mg, 0.237 mmole) was dissolved in acetonitrile (2 ml), and 1,8-diazabicyclo[5.4.0]-7-undecene (0.716 ml, 4.8 mmole) and isopropyl iodide (0.24 ml, 2.4 mmole) were added thereto and the mixture was stirred at room temperature for 16 hours. Then, the reaction mixture was treated following the procedure similar to that of Example 5, to yield 62 mg of the title compound 29' as a colorless oil (yield 64%).

Provenance & Evidence