Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Stannane, chlorotrioctadecyl- | HCID 301295 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86749217 | HCID 86749217 | 68.5% |
Reaction Steps
A mixture of 20.0 g of trioctadecyltin chloride, 3.0 g of sodium azide and 40 ml of toluene was stirred at 120° C. for 6 hours. After cooling, 100 ml of toluene was added to the reaction mixture. The toluene layer was washed with water, dried over magnesium sulfate and concentrated under reduced pressure to give 13.8 g of trioctadecyltin azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05599943 |
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| Source dataset | uspto-grants-1997_02 |
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| ORD ID | ord-50268ca960ab49cca717e03226b36b45 |
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| Source note | uspto-grants-1997_02 |
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