HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → 7-Methoxyheptanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 7-Bromoheptanoic acid | HCID 121723 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 7-Methoxyheptanoic Acid | HCID 15409528 | — |
Reaction Steps
The title compound was prepared by the method of Example 1 using 7-bromoheptanoic acid (50 g, 239 mmol) instead of 12-bromoundecanoic acid and dimethylformamide (300 mL) instead or methanol as the solvent. Concentration afforded the title compound (30 g) as a pale yellow liquid and the structure verified by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599947 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-a6e95cd702574fdb823077e48a9b60e0 |
| Source note | uspto-grants-1997_02 |