Benzoic Acid → HCID 86750280, compound

HRID 1449813Notes

Reaction equation

HRID 1449813 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH:8][CH2:9][CH:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[OH:11].[C:18](O)(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1.[C:27]([O:30]CC)(=[O:29])C.[CH3:33][OH:34]>>[OH:11][CH:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:9][NH:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][O:1][C:18](=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1.[C:27]([O-:30])(=[O:29])[C:33]([O-:1])=[O:34]

Participants

4

Reactant 3

HCID 243Benzoic AcidHCID 21584119Ethylacetate methanolHCID 54456417HCID 54456417, compound

Product 1

HCID 86750280HCID 86750280, compound

Procedure

According to method II from 2-(6-hydroxy-1-hexylamino)-1-phenylethanol and benzoic acid. Working up by means of chromatography (ethyl acetate/methanol 1:1). Recrystallized as the oxalate from acetone. Melting point: 121°-125° C.

Workup

  1. customRecrystallized as the oxalate from acetone

Sources & evidence

ORD record
ord-128dfd2f2e8649aea6ae130690bc8bbb
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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