HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → HCID 86750284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | Ethyl acetate methanol triethylamine | HCID 21980445 | — |
| Reactant | HCID 23352640 | HCID 23352640 | — |
| Product | HCID 86750284 | HCID 86750284 | — |
Reaction Steps
Preparation according to method II from 1-(2-chlorophenyl)-2-(6-hydroxy-1-hexylamino)ethanol and phenylacetic acid. Working up by means of chromatography (ethyl acetate/methanol/triethylamine 42.5:7.5:1.0). Recrystallized as the oxalate from acetone. Melting point: 114°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-31c4431269864ac9a872f543631ce051 |
| Source note | uspto-grants-1997_02 |