Benzenepropanoic acid → HCID 86750290, compound

HRID 1449820Notes

Reaction equation

HRID 1449820 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][NH:8][CH2:9][CH:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[OH:11].[C:18]1([CH2:24][CH2:25][C:26](O)=[O:27])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[C:29]([O:32]CC)(=[O:31])C.[CH3:35][OH:36]>>[OH:11][CH:10]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:9][NH:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][O:1][C:26](=[O:27])[CH2:25][CH2:24][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[C:29]([O-:32])(=[O:31])[C:35]([O-:1])=[O:36]

Participants

4

Reactant 3

HCID 107Benzenepropanoic acidHCID 21584119Ethylacetate methanolHCID 54456417HCID 54456417, compound

Product 1

HCID 86750290HCID 86750290, compound

Procedure

According to method II from 2-(6-hydroxy-1-hexylamino)-1-phenylethanol and 3-phenylpropionic acid. Working up by means of chromatography (ethyl acetate/methanol 1:1). Recrystallized as the oxalate from acetone. Melting point: 129°-133° C.

Workup

  1. customRecrystallized as the oxalate from acetone

Sources & evidence

ORD record
ord-c57660e1e2754ea3a23d2f9af9472d3d
Source dataset
uspto-grants-1997_02
Patent number
US05599966

Reaction notes

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