HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → HCID 54069235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 54093051 | HCID 54093051 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 54069235 | HCID 54069235 | — |
Reaction Steps
According to method I (tetrahydrofuran, reflux 4 days) from 2-amino-1-phenylethanol and (12-bromo-1-dodecyl)4-phenylbutanoate. Working up by means of chromatography (ethyl acetate/petroleum ether 60-80/triethylamine 6:4:1). Recrystallized from diethyl ether. Melting point: 73°-74° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-414e015e73db497199826b02b17ae626 |
| Source note | uspto-grants-1997_02 |