HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylethanolamine → HCID 86750291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Benzyl 6-bromohexanoate | HCID 562258 | — |
| Solvent | Ethyl acetate methanol triethylamine | HCID 21980445 | — |
| Product | HCID 86750291 | HCID 86750291 | — |
Reaction Steps
According to method I (tetrahydrofuran, reflux 4 days) from benzyl 6-bromohexanoate and 2-amino-1-phenylethanol. Working up by means of chromatography (ethyl acetate/methanol/triethylamine 3:1:0.1). Melting point: 77°-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-daf733f72c404b1bba8320e3cc75baf2 |
| Source note | uspto-grants-1997_02 |