HRID1449826

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8028

Tetrahydrofuran

C4H8O

HCID217242

2-Amino-1-(4-amino-3,5-dichlorophenyl)ethan-1-ol

C8H10Cl2N2O

HCID53734924

未命名化合物

PRODUCTS

生成物

结构：Nc1c(Cl)cc(C(O)CNCCCCCC(=O)OCCc2ccsc2)cc1Cl

HCID23352645

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID22036596

未命名化合物

PROCEDURE

实验过程

According to method I (tetrahydrofuran, reflux 4 days) from {2-(3-thienyl)ethyl}6-bromohexanoate and 2-amino-1-(4-amino-3,5-dichlorophenyl)ethanol. Working up by means of chromatography (ethyl acetate/triethylamine 8:1). Recrystallized as the base from diethyl ether. Melting point: 71°-73° C.

WORKUP

后处理

customRecrystallized as the base from diethyl ether