HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 86750295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Benzenemethanol, 4-amino-alpha-(aminomethyl)-3,5-dichloro- | HCID 217242 | — |
| Reactant | HCID 23352566 | HCID 23352566 | — |
| Solvent | Ethyl acetate triethylamine | HCID 22036596 | — |
| Product | HCID 86750295 | HCID 86750295 | — |
Reaction Steps
According to method I (dimethylformamide, 2 hours at 90° C.) from (6-bromo-1-hexyl)4-(4-methoxyphenyl)butanoate and 2-amino-1-(4-amino-3,5-dichlorophenyl)ethanol. Working up by means of chromatography (ethyl acetate/triethylamine 5:1). Recrystallized as the maleate from diethyl ether. Melting point: 66°-67° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05599966 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-239117809f6e47198a8b104810707a2f |
| Source note | uspto-grants-1997_02 |