HRID1450175

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)(C)OC(=O)N[C@H](CC1CCCCC1)C(=O)O

HCID2755927

N-(tert-Butoxycarbonyl)-3-cyclohexyl-D-alanine

C14H25NO4

HCID21226445

未命名化合物

结构：Cl.N=C(N)NCCC[C@@H](C=O)NC(=O)[C@@H]1CCCN1C(=O)[C@H](N)CC1CCCCC1.O

HCID178479447

未命名化合物

PRODUCTS

生成物

结构：Cl.N=C(N)NCCC[C@@H](C=O)NC(=O)[C@@H]1CCCN1C(=O)[C@H](N)CC1CCCCC1

HCID178479446

未命名化合物

PROCEDURE

实验过程

By methods substantially equivalent to those described in Example 1-A, 1-B, 1-C, 1-D, 1-H and 1-I, 2.14 g of NMI-D-Cha-Pro-Arg-H.HCl hydrate was prepared using Boc-D-Cha-OH in place of Boc-D-Phe-OH. Also, the tripeptide arginine lactam was reduced with LiAl(O-t-Bu)3H at -23° C. rather than LAH at -78° C.

WORKUP

后处理

customwas prepared