HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86750337, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 86750339 | HCID 86750339 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 86750337 | HCID 86750337 | — |
Reaction Steps
The title compound is prepared by the procedure of Example 18 using 0.387 g of product from Example 91, 0.046 g of sodium bicarbonate, 4 ml of water, 19 ml of dioxane, and 0.050 g of 10% palladium/carbon to give 0.031 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602118 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-997da81dbcc447479de744411e7c8830 |
| Source note | uspto-grants-1997_02 |