Hydrochloric Acid → HCID 178515941, compound

Participants

Reaction Conditions

Reaction Steps

2-Cyanophenol (1.19 g), ammonium chloride (0.695 g), and sodium azide (0.845 g) were added to dimethylformamide (5 ml). The mixture was heated with stirring at 120° C. for 3 h. After cooling, it was poured into ice water and acidified with dilute hydrochloric acid. The resulting crystals were collected by filtration and dried to give the title compound.

Provenance & Evidence