HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178447452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 178515941 | HCID 178515941 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178447452 | HCID 178447452 | — |
Reaction Steps
2-(1H-Tetrazol-5-yl)phenol (4.86 g) was dissolved in pyridine (20 ml), and pivaloyl chloride (7.2 g) was added to the solution at room temperature. After being stirred for 15 h, the mixture was poured into ice water and acidified with dilute hydrochloric acid. The resulting crystals were collected by filtration and dried to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05602161 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-cf1d4f3f3b2a4145a0a37baf75fff3d2 |
| Source note | uspto-grants-1997_02 |