Dicyclopentadiene → HCID 43754984, compound

Participants

Reaction Conditions

Reaction Steps

5-(t-butylanfinomethyl)norbomene. 14 g of dicyclopentadiene and 60 g of the N-allyl-N-t-butylamine were placed neat in a Parr High-Pressure Reactor. The reaction was heated to 185° C. with stirring for 15 h. The reaction was then cooled down and the reaction solution was distilled under vacuum (0.5 torr). The desired product distilled over at 35°-36 ° C. 24.6 g of product was collected in this way (64.7% yield).

Provenance & Evidence