Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cuminaldehyde | HCID 326 | — |
| Reactant | (4-Nitrophenyl)hydrazine | HCID 3310889 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 4504628 | HCID 4504628 | 92.1% |
Reaction Steps
In 20 ml of methanol was dissolved 3.06 g of 4-nitrophenylhydrazine. With 2.96 g of 4-isopropylbenzaldehyde added, the solution was refluxed at 100° C. for one hour. With the progress of reaction, crystals gradually precipitated. The crystals were collected by suction filtration, washed with methanol, and dried at 80° C. for 2 hours, obtaining 5.21 g (yield 92%) of pale yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05604004 |
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| Source dataset | uspto-grants-1997_02 |
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| ORD ID | ord-444292973dab40c89b31814cae0b4b8f |
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| Source note | uspto-grants-1997_02 |
|---|
