HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14647076, compound → HCID 136381075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14647076 | HCID 14647076 | — |
| Reactant | HCID 178458887 | HCID 178458887 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 136381075 | HCID 136381075 | 100% |
Reaction Steps
A mixture of 2.0 g (7.9 mmol) of 3-hydroxy-5-(1-methylthiocyclopropyl)-2-propionyl-2-cyclohexen-1-one, 1.8 g (9.0 mmol) of O-[4-trans-(4-chlorophenyl)-but-3-enyl]-hydroxylamine and 100 ml of methanol was stirred for 24 hours and then evaporated down under reduced pressure. Yield: 100%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604183 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-27439b0020a34633acf5c66e9d692632 |
| Source note | uspto-grants-1997_02 |