HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 5-Fluoro-2-nitrobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Fluoro-2-nitrobenzoic acid | HCID 2737420 | — |
| Product | 5-Fluoro-2-nitrobenzoyl chloride | HCID 15654868 | — |
Reaction Steps
A mixture of 5-fluoro-2-nitrobenzoic acid (47.51 g, 0.257 mol) and thionyl chloride (100 mL, 1.370 mol) is refluxed for several hours and concentrated in vacuo to give the title product which is used in Example 2 without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604180 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-3697ffb8d6ae47eaae98edc3f02bac4e |
| Source note | uspto-grants-1997_02 |