Diethylamine → HCID 19040686, compound

HRID 1451270Notes

Reaction equation

Cl[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[C:18]3[CH:19]=[C:20]4[O:25][CH2:24][O:23][C:21]4=[CH:22][C:17]=3[CH2:16][CH:15]([CH3:26])[N:14]([C:27](=[O:29])[CH3:28])[N:13]=2)=[CH:8][CH:7]=1)=[O:4].[CH2:30]([NH:32][CH2:33][CH3:34])[CH3:31]>>[CH2:30]([N:32]([CH2:33][CH3:34])[CH2:2][C:3]([NH:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[C:18]3[CH:19]=[C:20]4[O:25][CH2:24][O:23][C:21]4=[CH:22][C:17]=3[CH2:16][CH:15]([CH3:26])[N:14]([C:27](=[O:29])[CH3:28])[N:13]=2)=[CH:8][CH:7]=1)=[O:4])[CH3:31]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 53713423HCID 53713423, compound

Product 1

HCID 19040686HCID 19040686, compound

Procedure

It was prepared from 1-(4-chloroacetylaminophenyl)-3-acetyl-4-methyl-7,8-methylenedioxy-3,4-dihydro-5H-2,3-benzodiazepine and diethylamine by using the process described in Example 102, m.p.: 175°-176° C.

Sources & evidence

ORD record: ord-19c119ff28cc48a3870b23f0d111ebe0
Source dataset: uspto-grants-1997_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05604223

Reaction notes

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