HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23693686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 9803221 | HCID 9803221 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23693686 | HCID 23693686 | 99.8% |
Reaction Steps
A suspension of the acid from Step 5 (870 mg, 2.09 mmol) in 15 mL EtOH was treated with 1.00N NaOH (2.1 mL, 2.1 mmol), and stirred until the solid dissolved. The solution was concentrated to dryness, then dissolved in a minimum amount of water and freeze-dried to provide 914 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604253 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-8e6ecd6f863a414da6031f1c4ed8d289 |
| Source note | uspto-grants-1997_02 |