HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 22148996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 22148991 | HCID 22148991 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22148996 | HCID 22148996 | — |
Reaction Steps
To a solution of the compound from Example 1 (75 mg, 0.19 mmol) in 10 mL EtOAc was added ethereal diazomethane solution until a yellow colour persisted. The solution was concentrated in vacuo and crystalized from ether/hexanes to provide 67 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05604253 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-23bdc2ce63ed4907bd9cbc0368be09df |
| Source note | uspto-grants-1997_02 |