HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15200703, compound → HCID 19972869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15200703 | HCID 15200703 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 19972869 | HCID 19972869 | 80% |
Reaction Steps
A solution of 25 mg (0.07 mmol) of 3 in xylene (60 ml) was refluxed for 16 hours while air was bubbling through the solution. After evaporation of the solvent, the residue was purified by silica gel chromatography, using ethyl acetate as eluent to yield 20 mg (80%) of 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05605905 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-91b37fa60f194ae0b03532e900609a18 |
| Source note | uspto-grants-1997_02 |