2-Butanethiol → Dibutan-2-yl disulfide
Reaction equation
[CH3:1][CH:2]([SH:5])[CH2:3][CH3:4]>C(#N)C>[CH3:1][CH:2]([S:5][S:5][CH:2]([CH3:1])[CH2:3][CH3:4])[CH2:3][CH3:4]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 150 μg of LL-E33288γ1 -I in 1 ml of acetonitrile was treated with 50 μl of a 1 μmole/ml solution of 1-methyl-1-propyl mercaptan. After 2 hours, the reaction was complete, giving the desired 1-methyl-1-propyl disulfide of LL-E33288γ1 -I.
Sources & evidence
- ORD record
- ord-c15de9c81da446228f35a93da269be60
- Source dataset
- uspto-grants-1997_02
- Patent number
- US05606040
Reaction notes
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