HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butanethiol → Dibutan-2-yl disulfide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butanethiol | HCID 10560 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Dibutan-2-yl disulfide | HCID 94314 | — |
Reaction Steps
A solution of 150 μg of LL-E33288γ1 -I in 1 ml of acetonitrile was treated with 50 μl of a 1 μmole/ml solution of 1-methyl-1-propyl mercaptan. After 2 hours, the reaction was complete, giving the desired 1-methyl-1-propyl disulfide of LL-E33288γ1 -I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05606040 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-c15de9c81da446228f35a93da269be60 |
| Source note | uspto-grants-1997_02 |