反应详情

To 10 g of 8-acetoxy-5,6,7,8-tetrahydroquinoline in 30 mL of methanol was added 30 mL of 30% sodium hydroxide in water. The mixture was heated to reflux for 2 min and the methanol was removed in vacuo. The residual organic product was extracted with chloroform. The chloroform extracts were dried over sodium sulfate and evaporation of the solvent gave 8 g of product as an oil, characterized by its NMR.

1. temperatureThe mixture was heated
2. temperatureto reflux for 2 min
3. customthe methanol was removed in vacuo
4. extractionThe residual organic product was extracted with chloroform
5. dry with materialThe chloroform extracts were dried over sodium sulfate and evaporation of the solvent