HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 86750390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 2-(Pyridin-4-yl)-methylene-indan-1-one | HCID 19973473 | — |
| Product | HCID 86750390 | HCID 86750390 | — |
Reaction Steps
##STR7## 10 g of compound from Example 1 were dissolved in 150 ml of boiling acetonitrile and 7.5 g of benzyl bromide were added hot. The mixture was heated to boiling under reflux for a further 2 h, the product precipitating. It was allowed to cool, and the resulting precipitate was filtered off with suction, washed with acetonitrile and methyl tert-butyl ether in the sequence indicated and dried in air.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05606064 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-e0253da9fe84418f975b0382938190b4 |
| Source note | uspto-grants-1997_02 |