HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19973449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19973434 | HCID 19973434 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19973449 | HCID 19973449 | — |
Reaction Steps
6.80 g of the 2-methylimidazo-[1,2-a]pyridine-6-methanol prepared in the Preparative Example 16 was dissolved in 90 ml of chloroform, followed by the dropwise addition of 6.1 ml of thionyl chloride under stirring at room temperature. After 2 hours, the solvent was distilled off. Crude 6-chloromethyl-2methylimidazo-[1,2-a]pyridine hydrochloride was obtained as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05606061 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-d68fb8fe4ccd4e2a87e4aac04f1400b6 |
| Source note | uspto-grants-1997_02 |