HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19972426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 19972449 | HCID 19972449 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19972426 | HCID 19972426 | 69.7% |
Reaction Steps
A solution of 9.2 g of Intermediate III and 7.8 g of thionyl chloride in 75 ml of toluene was refluxed for 3 hours. After cooling to 20°-25° C. the resultant crystal was collected by suction filtration, washed with acetone and dried in vacuo to give 6.8 g of the title compound, m.p. (190) 196°-198° C. after recrystallization from toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05605896 |
| Source dataset | uspto-grants-1997_02 |
| ORD ID | ord-910531e11a7041eaa0f5c88e8db6a1e4 |
| Source note | uspto-grants-1997_02 |