HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57526844, compound → HCID 57526804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57526844 | HCID 57526844 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 57526804 | HCID 57526804 | — |
Reaction Steps
tert-Butyl(S)-3-{10-[tert-butoxycarbonyl-(4-ethoxyphenyl)amino]-6,9-dihydro-1,4,5,10a-tetraazacyclohepta[f]inden-5-yl}piperidine-1-carboxylate (12.5 mg) was hydrogenated in the presence of palladium-carbon (15 mg) in ethanol (1.2 mL) under a hydrogen atmosphere. After the reaction, the palladium-carbon was filtered off, and the filtrate was concentrated. The residue was used for the subsequent reaction without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07473694B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-79e18c62ba56475fa1119949fcba6812 |
| Source note | uspto-grants-2009_01 |