化工社化工社 化学情報印刷レポート · 研究参考用
Methanesulfonyl chloride → 3-methylsulfonylamino-5-nitro-1H-indazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanesulfonyl chloride | HCID 31297 | — |
| 反応物 | 3-Amino-5-nitroindazole | HCID 3136655 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 3-methylsulfonylamino-5-nitro-1H-indazole | HCID 22567201 | 84.4% |
反応手順
3-Methylsulfonylamino-5-nitro-1H-indazole can be obtained as described in Example 2 from 0.7 g of 3-amino-5-nitro-1H-indazole, 23 ml of pyridine and 0.455 g of methylsulfonyl chloride. 0.85 g of 3-methylsulfonylamino-5-nitro-1H-indazole is thus obtained in the form of an orange powder used as it is in the following step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07473701B2 |
| 出典データセット | uspto-grants-2009_01 |
| ORD ID | ord-258781a826894dd9831e0358f5a3dd02 |
| 出典メモ | uspto-grants-2009_01 |