4-Bromo-2-ethylphenol → HCID 58762505, compound

HRID 1453064Notes

Reaction equation

HRID 1453064 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[C:4]([CH:9]([CH3:11])[CH3:10])[CH:3]=1.BrC1C=C[C:16]([OH:19])=[C:15](CC)C=1>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][C:16](=[O:19])[CH3:15])=[C:4]([CH:9]([CH3:11])[CH3:10])[CH:3]=1

Participants

3

Reactant 2

HCID 878774-Bromo-2-ethylphenolHCID 147934824-Bromo-2-(propan-2-yl)phenol

Product 1

HCID 58762505HCID 58762505, compound

Procedure

The title compound was prepared as described in Step 2 of Example A(22) where 4-Bromo-2-isopropyl-phenol from step 1, was substituted in place of 4-Bromo-2-ethyl-phenol. 1H NMR (CDCl3): δ 1.20 (d, 6H, J=7.1 Hz), 2.32 (s, 3H), 2.98 (m, 1H), 6.88 (d, 1H, J=8.6 Hz), 7.31 (dd, 1H, J=8.6, 2.3 Hz), 7.41 (d, 1H, J=2.5 Hz).

Sources & evidence

ORD record
ord-0ee5b85354074fbe94dbb4e26334df0c
Source dataset
uspto-grants-2009_01
Patent number
US07473790B2

Reaction notes

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