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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1453284Generated: October 26, 2026

3-Ethoxy-2-methylacrylaldehyde → HCID 178430151, compound

https://huagongshe.com/reaction/1453284

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Ethoxy-2-methylacrylaldehydeHCID 3084868—
Reactant5-amino-1H-1,2,4-triazole-3-thiolHCID 178509296—
ProductHCID 178430151HCID 178430151—

Reaction Steps

The title compound was prepared from 3-ethoxymethacrolein and 3-amino-5-mercapto-1,2,4-triazole as previously described by M. Kunstlinger and E. Breitmaier in Synthesis, 1983, 44-47. 1H NMR (DMSO-d6) d 2.31 (s, 1H) 8.45 (s, 1H) 8.68 (s, 1H). MS (APCI) calcd for C6H6N4S: 166.21; found (M+H+) 167.0.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07473790B2
Source datasetuspto-grants-2009_01
ORD IDord-198a000b1b9648e1b5598f03f6cda602
Source noteuspto-grants-2009_01